Crystallography Open Database

Information card for entry 4085347

Preview

Coordinates	4085347.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Motis-287 (Sara)
Formula	C28 H48 Cl2 N6 Si2 U
Calculated formula	C28 H48 Cl2 N6 Si2 U
SMILES	[U]1234(Cl)(Cl)([N](=C(N1[Si](C)(C)C)c1ccccc1)CC[N]2(C)C)[N](=C(N3[Si](C)(C)C)c1ccccc1)CC[N]4(C)C
Title of publication	Actinide Amidinate Complexes with a Dimethylamine Side Arm: Synthesis, Structural Characterization, and Reactivity
Authors of publication	Karmel, Isabell S. R.; Fridman, Natalia; Eisen, Moris S.
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	3
Pages of publication	636
a	8.4 ± 0.002 Å
b	14.467 ± 0.003 Å
c	15.763 ± 0.003 Å
α	98.11 ± 0.03°
β	104.33 ± 0.03°
γ	104.46 ± 0.03°
Cell volume	1754.6 ± 0.8 Å³
Cell temperature	240 ± 2 K
Ambient diffraction temperature	240 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1039
Residual factor for significantly intense reflections	0.0864
Weighted residual factors for significantly intense reflections	0.2324
Weighted residual factors for all reflections included in the refinement	0.243
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178742 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/53.	4085347.cif
132973	2015-03-04	cif/ Updating files of 4085347, 4085348, 4085349 Original log message: Adding full bibliography for 4085347--4085349.cif.	4085347.cif
130841	2015-02-04	cif/ Adding structures of 4085347, 4085348, 4085349 via cif-deposit CGI script.	4085347.cif