Crystallography Open Database

Information card for entry 4087971

Preview

Coordinates	4087971.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[PhSn(CH2Me2SiO)(μ3-O)Sn(μ-OH)t-Bu2]2
Formula	C34 H64 O6 Si2 Sn4
Calculated formula	C34 H64 O6 Si2 Sn4
SMILES	C1[Si](C)(C)O[Sn]2([O]3[Sn]41([O]1[Sn]([OH]4)(C(C)(C)C)(O[Si](C[Sn]31([OH]2)c1ccccc1)(C)C)C(C)(C)C)c1ccccc1)(C(C)(C)C)C(C)(C)C
Title of publication	cyclo-Stannasiloxanes Containing both Oxygen Atoms and Methylene Moieties within the Ring and Formation of Related Organotin Oxo Clusters
Authors of publication	Baba Haj, Samer; Dietz, Christina; Lutter, Michael; Jurkschat, Klaus
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	23
Pages of publication	5555
a	14.2431 ± 0.0005 Å
b	10.4123 ± 0.0003 Å
c	15.5313 ± 0.0005 Å
α	90°
β	106.366 ± 0.003°
γ	90°
Cell volume	2210.02 ± 0.13 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0308
Residual factor for significantly intense reflections	0.0197
Weighted residual factors for significantly intense reflections	0.0393
Weighted residual factors for all reflections included in the refinement	0.0403
Goodness-of-fit parameter for all reflections included in the refinement	0.897
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
237162 (current)	2019-11-24	cif/ Adding structures of 4087968, 4087969, 4087970, 4087971, 4087972 via cif-deposit CGI script.	4087971.cif