Crystallography Open Database

Information card for entry 4087972

Preview

Coordinates	4087972.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[(t-Bu2)(μ-OH)Sn(μ3-O)Sn(Ph)(CH2Me2SiO)Sn(t-Bu2)(μ3-O)]2
Formula	C50 H100 O8 Si2 Sn6
Calculated formula	C50 H100 O8 Si2 Sn6
Title of publication	cyclo-Stannasiloxanes Containing both Oxygen Atoms and Methylene Moieties within the Ring and Formation of Related Organotin Oxo Clusters
Authors of publication	Baba Haj, Samer; Dietz, Christina; Lutter, Michael; Jurkschat, Klaus
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	23
Pages of publication	5555
a	9.9649 ± 0.0007 Å
b	28.0445 ± 0.0011 Å
c	12.2933 ± 0.0007 Å
α	90°
β	112.096 ± 0.007°
γ	90°
Cell volume	3183.2 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0512
Residual factor for significantly intense reflections	0.029
Weighted residual factors for significantly intense reflections	0.051
Weighted residual factors for all reflections included in the refinement	0.0526
Goodness-of-fit parameter for all reflections included in the refinement	0.839
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
237162 (current)	2019-11-24	cif/ Adding structures of 4087968, 4087969, 4087970, 4087971, 4087972 via cif-deposit CGI script.	4087972.cif