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Information card for entry 4088022
Preview
| Coordinates | 4088022.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H33 F2 Ni O3 P3 |
|---|---|
| Calculated formula | C30 H33 F2 Ni O3 P3 |
| Title of publication | d10 Nickel Difluorocarbenes and Their Cycloaddition Reactions with Tetrafluoroethylene |
| Authors of publication | Harrison, Daniel J.; Daniels, Alex L.; Korobkov, Ilia; Baker, R. Tom |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 24 |
| Pages of publication | 5683 |
| a | 10.4679 ± 0.0003 Å |
| b | 11.661 ± 0.0003 Å |
| c | 24.7749 ± 0.0008 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3024.18 ± 0.15 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0644 |
| Residual factor for significantly intense reflections | 0.0396 |
| Weighted residual factors for significantly intense reflections | 0.0716 |
| Weighted residual factors for all reflections included in the refinement | 0.078 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237220 (current) | 2019-11-24 | cif/ Adding structures of 4088022 via cif-deposit CGI script. |
4088022.cif |
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Users of the data should acknowledge the original authors of the
structural data.