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Information card for entry 4088024
Preview
| Coordinates | 4088024.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C48 H59 B3 Cl2 F12 N7 P2 Rh |
|---|---|
| Calculated formula | C45 H54 B3 F12 N6 P2 Rh |
| Title of publication | Synthesis, Isomerization, and Catalytic Transfer Hydrogenation Activity of Rhodium(III) Complexes Containing Both Chelating Dicarbenes and Diphosphine Ligands |
| Authors of publication | Farrell, Kevin; Müller-Bunz, Helge; Albrecht, Martin |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 24 |
| Pages of publication | 5723 |
| a | 13.3773 ± 0.0001 Å |
| b | 24.026 ± 0.0003 Å |
| c | 16.9704 ± 0.0002 Å |
| α | 90° |
| β | 97.94 ± 0.0008° |
| γ | 90° |
| Cell volume | 5402.05 ± 0.1 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.0389 |
| Residual factor for significantly intense reflections | 0.0385 |
| Weighted residual factors for significantly intense reflections | 0.1012 |
| Weighted residual factors for all reflections included in the refinement | 0.1016 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237222 (current) | 2019-11-24 | cif/ Adding structures of 4088023, 4088024, 4088025, 4088026 via cif-deposit CGI script. |
4088024.cif |
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Users of the data should acknowledge the original authors of the
structural data.