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Information card for entry 4089653
Preview
| Coordinates | 4089653.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C65.5 H61 B Cl F24 N6 O6 Rh |
|---|---|
| Calculated formula | C65.5 H61 B Cl F24 N6 O6 Rh |
| Title of publication | Rhodium(I) Complexes of the Conformationally Rigid IBioxMe4 Ligand: Isolation of a Stable Low-Coordinate T-Shaped Complex |
| Authors of publication | Chaplin, Adrian B. |
| Journal of publication | Organometallics |
| Year of publication | 2014 |
| Journal volume | 33 |
| Journal issue | 3 |
| Pages of publication | 624 |
| a | 14.6083 ± 0.0003 Å |
| b | 18.2307 ± 0.0004 Å |
| c | 28.3089 ± 0.0005 Å |
| α | 99.6629 ± 0.0016° |
| β | 91.5109 ± 0.0016° |
| γ | 107.281 ± 0.0019° |
| Cell volume | 7073.4 ± 0.3 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0683 |
| Residual factor for significantly intense reflections | 0.0507 |
| Weighted residual factors for significantly intense reflections | 0.1213 |
| Weighted residual factors for all reflections included in the refinement | 0.1307 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243714 (current) | 2019-11-26 | cif/ Adding structures of 4089653, 4089654 via cif-deposit CGI script. |
4089653.cif |
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Users of the data should acknowledge the original authors of the
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