Crystallography Open Database

Information card for entry 4106073

Preview

Coordinates	4106073.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(Rb(18-crown-6))2[SbGe7-Ge7Sb] 1en
Formula	C26 H56 Ge7 N2 O12 Rb2 Sb2
Calculated formula	C26 H56 Ge6.99 N2 O12 Rb2 Sb2.01
Title of publication	"n-Doping" of Deltahedral Zintl Ions
Authors of publication	Miriam M. Gillett-Kunnath; Allen G. Oliver; Slavi C. Sevov
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	6560 - 6562
a	33.1657 ± 0.0018 Å
b	13.9299 ± 0.0007 Å
c	10.5431 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	4870.9 ± 0.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0861
Residual factor for significantly intense reflections	0.0736
Weighted residual factors for significantly intense reflections	0.1713
Weighted residual factors for all reflections included in the refinement	0.1796
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178806 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/60.	4106073.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4106073.cif
52863	2012-04-16	../uploads/cif-deposit/cod/cif Adding structures of 4106073 via cif-deposit CGI script.	4106073.cif