Crystallography Open Database

Information card for entry 4106074

Preview

Coordinates	4106074.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(K-crypt)2[SbGe8-SbPh2]
Formula	C48 H82 Ge8 K2 N4 O12 Sb2
Calculated formula	C48 H82 Ge8 K2 N4 O12 Sb2
Title of publication	"n-Doping" of Deltahedral Zintl Ions
Authors of publication	Miriam M. Gillett-Kunnath; Allen G. Oliver; Slavi C. Sevov
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	6560 - 6562
a	12.9472 ± 0.0009 Å
b	16.5696 ± 0.0009 Å
c	16.5832 ± 0.0009 Å
α	81.879 ± 0.003°
β	69.709 ± 0.002°
γ	84.921 ± 0.003°
Cell volume	3300.4 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0646
Residual factor for significantly intense reflections	0.0462
Weighted residual factors for significantly intense reflections	0.1019
Weighted residual factors for all reflections included in the refinement	0.1133
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178806 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/60.	4106074.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4106074.cif
52864	2012-04-16	../uploads/cif-deposit/cod/cif Adding structures of 4106074 via cif-deposit CGI script.	4106074.cif