Crystallography Open Database

Information card for entry 4107207

Preview

Coordinates	4107207.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H55 Br N2 Si
Calculated formula	C39 H55 Br N2 Si
Title of publication	Room-Temperature Dissociation of 1,2-Dibromodisilenes to Bromosilylenes
Authors of publication	Katsunori Suzuki; Tsukasa Matsuo; Daisuke Hashizume; Kohei Tamao
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	19710 - 19713
a	19.547 ± 0.003 Å
b	12.545 ± 0.0019 Å
c	14.345 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	3517.6 ± 0.9 Å³
Cell temperature	153 K
Ambient diffraction temperature	153 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0549
Residual factor for significantly intense reflections	0.0408
Weighted residual factors for significantly intense reflections	0.0769
Weighted residual factors for all reflections included in the refinement	0.0833
Goodness-of-fit parameter for all reflections included in the refinement	0.97
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178818 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/72.	4107207.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4107207.cif
54859	2012-04-30	cif/ Adding structures of 4107207 via cif-deposit CGI script.	4107207.cif