Crystallography Open Database

Information card for entry 4107208

Preview

Coordinates	4107208.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H55 Br Si3
Calculated formula	C32 H55 Br Si3
Title of publication	Room-Temperature Dissociation of 1,2-Dibromodisilenes to Bromosilylenes
Authors of publication	Katsunori Suzuki; Tsukasa Matsuo; Daisuke Hashizume; Kohei Tamao
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	19710 - 19713
a	21.785 ± 0.003 Å
b	12.4724 ± 0.0015 Å
c	25.669 ± 0.003 Å
α	90°
β	98.697 ± 0.002°
γ	90°
Cell volume	6894.4 ± 1.5 Å³
Cell temperature	223 K
Ambient diffraction temperature	223 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1105
Residual factor for significantly intense reflections	0.0694
Weighted residual factors for significantly intense reflections	0.1738
Weighted residual factors for all reflections included in the refinement	0.1992
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178818 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/72.	4107208.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4107208.cif
54860	2012-04-30	cif/ Adding structures of 4107208 via cif-deposit CGI script.	4107208.cif