Crystallography Open Database

Information card for entry 4112900

Preview

Coordinates	4112900.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Li(THF)3(Et2O)][Li(HGeDipp*)2]
Formula	C76 H98 Ge2 Li2 O4
Calculated formula	C78 H98 Ge2 Li2 O4
Title of publication	Reduction of Digermenes with Alkali Metals: Salts of Formula M2[{Ge(H)Ar'}2] (M = Li, Na, or K, Ar' = Terphenyl) with Three Different Structures
Authors of publication	Anne F. Richards; Marcin Brynda; Philip P. Power
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	10530 - 10531
a	18.6448 ± 0.0014 Å
b	17.6953 ± 0.0014 Å
c	12.6498 ± 0.001 Å
α	90°
β	114.431 ± 0.001°
γ	90°
Cell volume	3799.8 ± 0.5 Å³
Cell temperature	91 ± 2 K
Ambient diffraction temperature	91 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0996
Residual factor for significantly intense reflections	0.0866
Weighted residual factors for significantly intense reflections	0.2484
Weighted residual factors for all reflections included in the refinement	0.2612
Goodness-of-fit parameter for all reflections included in the refinement	1.092
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178900 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/29.	4112900.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4112900.cif
65318	2012-09-05	cif/ Adding structures of 4112900 via cif-deposit CGI script.	4112900.cif