Crystallography Open Database

Information card for entry 4112901

Preview

Coordinates	4112901.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[(Dipp*GeH2)]K2
Formula	C60 H76 Ge2 K2
Calculated formula	C60 H76 Ge2 K2
Title of publication	Reduction of Digermenes with Alkali Metals: Salts of Formula M2[{Ge(H)Ar'}2] (M = Li, Na, or K, Ar' = Terphenyl) with Three Different Structures
Authors of publication	Anne F. Richards; Marcin Brynda; Philip P. Power
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	10530 - 10531
a	11.4599 ± 0.0011 Å
b	18.3736 ± 0.0018 Å
c	13.3713 ± 0.0013 Å
α	90°
β	101.959 ± 0.002°
γ	90°
Cell volume	2754.3 ± 0.5 Å³
Cell temperature	91 ± 2 K
Ambient diffraction temperature	91 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.038
Residual factor for significantly intense reflections	0.0304
Weighted residual factors for significantly intense reflections	0.0781
Weighted residual factors for all reflections included in the refinement	0.0848
Goodness-of-fit parameter for all reflections included in the refinement	0.875
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178900 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/29.	4112901.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4112901.cif
65319	2012-09-05	cif/ Adding structures of 4112901 via cif-deposit CGI script.	4112901.cif