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Information card for entry 4115172
Preview
| Coordinates | 4115172.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C16 H31 Ge Li O Si2 |
|---|---|
| Calculated formula | C16 H39 Ge Li O Si2 |
| Title of publication | Sila-metalation Route to Hydrido(trialkylsilyl)silyllithiums |
| Authors of publication | Takeaki Iwamoto; Junichiro Okita; Chizuko Kabuto; Mitsuo Kira |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2002 |
| Journal volume | 124 |
| Pages of publication | 11604 - 11605 |
| a | 11.88 ± 0.002 Å |
| b | 15.941 ± 0.002 Å |
| c | 12.802 ± 0.001 Å |
| α | 90° |
| β | 107.25 ± 0.0009° |
| γ | 90° |
| Cell volume | 2315.4 ± 0.5 Å3 |
| Cell temperature | 123.2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.0448 |
| Weighted residual factors for all reflections included in the refinement | 0.1217 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.906 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4115172.cif |
| 120077 | 2014-07-12 | Adding DOIs to range 4/11 structures. | 4115172.cif |
| 68602 | 2012-11-08 | cif/ Adding structures of 4115172 via cif-deposit CGI script. |
4115172.cif |
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Users of the data should acknowledge the original authors of the
structural data.