Crystallography Open Database

Information card for entry 4115173

Preview

Coordinates	4115173.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H78 Li2 O2 Si6
Calculated formula	C32 H78 Li2 O2 Si6
Title of publication	Sila-metalation Route to Hydrido(trialkylsilyl)silyllithiums
Authors of publication	Takeaki Iwamoto; Junichiro Okita; Chizuko Kabuto; Mitsuo Kira
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	11604 - 11605
a	11.8427 ± 0.0004 Å
b	15.943 ± 0.001 Å
c	12.77 ± 0.0004 Å
α	90°
β	107.467 ± 0.004°
γ	90°
Cell volume	2299.91 ± 0.19 Å³
Cell temperature	150.2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0743
Residual factor for significantly intense reflections	0.0548
Weighted residual factors for significantly intense reflections	0.1456
Weighted residual factors for all reflections included in the refinement	0.1615
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4115173.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115173.cif
68603	2012-11-08	cif/ Adding structures of 4115173 via cif-deposit CGI script.	4115173.cif