Crystallography Open Database

Information card for entry 4122106

Preview

Coordinates	4122106.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 F23 O3 S Sb
Calculated formula	C25 F23 O3 S Sb
SMILES	[Sb](c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)OS(=O)(=O)C(F)(F)F
Title of publication	[Sb(C6F5)4][B(C6F5)4]: An Air Stable, Lewis Acidic Stibonium Salt That Activates Strong Element-Fluorine Bonds.
Authors of publication	Pan, Baofei; Gabbaï, François P
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	27
Pages of publication	9564 - 9567
a	17.66 ± 0.002 Å
b	20.429 ± 0.003 Å
c	15.602 ± 0.002 Å
α	90°
β	93.314 ± 0.002°
γ	90°
Cell volume	5619.4 ± 1.3 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.0388
Weighted residual factors for significantly intense reflections	0.1202
Weighted residual factors for all reflections included in the refinement	0.1363
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179023 (current)	2016-03-22	cif/4/12/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/12/21.	4122106.cif
121261	2014-08-05	cif/ Updating files of 4122105, 4122106, 4122107 Original log message: Adding full bibliography for 4122105--4122107.cif.	4122106.cif
118248	2014-06-28	cif/ Adding structures of 4122105, 4122106, 4122107 via cif-deposit CGI script.	4122106.cif