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Information card for entry 4125753
Preview
| Coordinates | 4125753.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | Pd-complx |
|---|---|
| Formula | C26 H21 F3 N4 O5 Pd S |
| Calculated formula | C26 H21 F3 N4 O5 Pd S |
| Title of publication | Reductive C(sp(2))-N Elimination from Isolated Pd(IV) Amido Aryl Complexes Prepared Using H2O2 as Oxidant. |
| Authors of publication | Abada, Elikplim; Zavalij, Peter Y.; Vedernikov, Andrei N. |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2017 |
| Journal volume | 139 |
| Journal issue | 2 |
| Pages of publication | 643 - 646 |
| a | 13.1494 ± 0.0007 Å |
| b | 12.7371 ± 0.0007 Å |
| c | 31.5681 ± 0.0016 Å |
| α | 90° |
| β | 101.788 ± 0.0012° |
| γ | 90° |
| Cell volume | 5175.7 ± 0.5 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0465 |
| Residual factor for significantly intense reflections | 0.0308 |
| Weighted residual factors for significantly intense reflections | 0.0638 |
| Weighted residual factors for all reflections included in the refinement | 0.0697 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 193129 (current) | 2017-03-04 | cif/ Adding structures of 4125753 via cif-deposit CGI script. |
4125753.cif |
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