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Information card for entry 4125754
Preview
| Coordinates | 4125754.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Pd-complex |
|---|---|
| Chemical name | Pd-complex |
| Formula | C28 H29 N3 O6 Pd S |
| Calculated formula | C28 H29 N3 O6 Pd S |
| Title of publication | Reductive C(sp(2))-N Elimination from Isolated Pd(IV) Amido Aryl Complexes Prepared Using H2O2 as Oxidant. |
| Authors of publication | Abada, Elikplim; Zavalij, Peter Y.; Vedernikov, Andrei N. |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2017 |
| Journal volume | 139 |
| Journal issue | 2 |
| Pages of publication | 643 - 646 |
| a | 30.3195 ± 0.0017 Å |
| b | 11.3339 ± 0.0006 Å |
| c | 17.6574 ± 0.001 Å |
| α | 90° |
| β | 118.758 ± 0.0008° |
| γ | 90° |
| Cell volume | 5319.4 ± 0.5 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0438 |
| Residual factor for significantly intense reflections | 0.0336 |
| Weighted residual factors for significantly intense reflections | 0.0659 |
| Weighted residual factors for all reflections included in the refinement | 0.0685 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.387 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 193130 (current) | 2017-03-04 | cif/ Adding structures of 4125754 via cif-deposit CGI script. |
4125754.cif |
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