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Information card for entry 4127742
Preview
| Coordinates | 4127742.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C53 H78 N4 O5 Si3 |
|---|---|
| Calculated formula | C53 H78 N4 O5 Si3 |
| Title of publication | Synthesis of an Isolable Bis(silylene)-Stabilized Silylone and Its Reactivity Toward Small Gaseous Molecules. |
| Authors of publication | Wang, Yuwen; Karni, Miriam; Yao, Shenglai; Kaushansky, Alexander; Apeloig, Yitzhak; Driess, Matthias |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2019 |
| Journal volume | 141 |
| Journal issue | 32 |
| Pages of publication | 12916 - 12927 |
| a | 13.9968 ± 0.001 Å |
| b | 15.1411 ± 0.0013 Å |
| c | 15.8329 ± 0.0009 Å |
| α | 61.805 ± 0.007° |
| β | 65.984 ± 0.006° |
| γ | 68.07 ± 0.007° |
| Cell volume | 2632 ± 0.4 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1004 |
| Residual factor for significantly intense reflections | 0.0559 |
| Weighted residual factors for significantly intense reflections | 0.1284 |
| Weighted residual factors for all reflections included in the refinement | 0.1597 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 220917 (current) | 2019-11-02 | cif/ Adding structures of 4127739, 4127740, 4127741, 4127742, 4127743, 4127744, 4127745, 4127746 via cif-deposit CGI script. |
4127742.cif |
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Users of the data should acknowledge the original authors of the
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