Crystallography Open Database

Information card for entry 4128327

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Coordinates	4128327.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C229 H96 Au24 Cl2 F108 P2 Pt
Calculated formula	C229 H96 Au24 Cl2 F108 P2 Pt
Title of publication	Efficient and Selective Conversion of Phosphine-Protected (MAu<sub>8</sub>)<sup>2+</sup> (M = Pd, Pt) Superatoms to Thiolate-Protected (MAu<sub>12</sub>)<sup>6+</sup> or Alkynyl-Protected (MAu<sub>12</sub>)<sup>4+</sup> Superatoms via Hydride Doping.
Authors of publication	Takano, Shinjiro; Ito, Shun; Tsukuda, Tatsuya
Journal of publication	Journal of the American Chemical Society
Year of publication	2019
Journal volume	141
Journal issue	40
Pages of publication	15994 - 16002
a	17.464 ± 0.003 Å
b	20.626 ± 0.004 Å
c	35.907 ± 0.007 Å
α	90°
β	95.69 ± 0.003°
γ	90°
Cell volume	12870 ± 4 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	7
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0699
Residual factor for significantly intense reflections	0.0627
Weighted residual factors for significantly intense reflections	0.1612
Weighted residual factors for all reflections included in the refinement	0.1668
Goodness-of-fit parameter for all reflections included in the refinement	1.122
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
221450 (current)	2019-11-03	cif/ Adding structures of 4128327 via cif-deposit CGI script.	4128327.cif