Crystallography Open Database

Information card for entry 4128328

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Coordinates	4128328.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H198 Au24 Pt S18 Si18
Calculated formula	C72 H198 Au24 Pt S18 Si18
Title of publication	Efficient and Selective Conversion of Phosphine-Protected (MAu<sub>8</sub>)<sup>2+</sup> (M = Pd, Pt) Superatoms to Thiolate-Protected (MAu<sub>12</sub>)<sup>6+</sup> or Alkynyl-Protected (MAu<sub>12</sub>)<sup>4+</sup> Superatoms via Hydride Doping.
Authors of publication	Takano, Shinjiro; Ito, Shun; Tsukuda, Tatsuya
Journal of publication	Journal of the American Chemical Society
Year of publication	2019
Journal volume	141
Journal issue	40
Pages of publication	15994 - 16002
a	16.883 ± 0.003 Å
b	16.927 ± 0.003 Å
c	17.005 ± 0.003 Å
α	103.829 ± 0.001°
β	112.014 ± 0.001°
γ	107.241 ± 0.001°
Cell volume	3952.2 ± 1.2 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.044
Residual factor for significantly intense reflections	0.0355
Weighted residual factors for significantly intense reflections	0.0604
Weighted residual factors for all reflections included in the refinement	0.0638
Goodness-of-fit parameter for all reflections included in the refinement	0.971
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
221451 (current)	2019-11-03	cif/ Adding structures of 4128328 via cif-deposit CGI script.	4128328.cif