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Information card for entry 4133556
Preview
| Coordinates | 4133556.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H45 Li N8 Si0.97 |
|---|---|
| Calculated formula | C36 H45 Li N8 Si0.9685 |
| Title of publication | Calix[4]pyrrole Hydridosilicate: The Elusive Planar Tetracoordinate Silicon Imparts Striking Stability to Its Anionic Silicon Hydride. |
| Authors of publication | Ebner, Fabian; Greb, Lutz |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2018 |
| Journal volume | 140 |
| Journal issue | 50 |
| Pages of publication | 17409 - 17412 |
| a | 10.729 ± 0.002 Å |
| b | 20.345 ± 0.004 Å |
| c | 16.436 ± 0.003 Å |
| α | 90° |
| β | 90.71 ± 0.03° |
| γ | 90° |
| Cell volume | 3587.4 ± 1.2 Å3 |
| Cell temperature | 120 K |
| Ambient diffraction temperature | 120 K |
| Number of distinct elements | 5 |
| Space group number | 7 |
| Hermann-Mauguin space group symbol | P 1 n 1 |
| Hall space group symbol | P -2yac |
| Residual factor for all reflections | 0.1132 |
| Residual factor for significantly intense reflections | 0.0543 |
| Weighted residual factors for significantly intense reflections | 0.0968 |
| Weighted residual factors for all reflections included in the refinement | 0.1157 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.006 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243313 (current) | 2019-11-26 | cif/ Adding structures of 4133556 via cif-deposit CGI script. |
4133556.cif |
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