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Information card for entry 4133557
Preview
Coordinates | 4133557.cif |
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Original paper (by DOI) | HTML |
Formula | C29 H34 Cl2 K N4 Si |
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Calculated formula | C29 H34 Cl2 K N4 Si |
Title of publication | Calix[4]pyrrole Hydridosilicate: The Elusive Planar Tetracoordinate Silicon Imparts Striking Stability to Its Anionic Silicon Hydride. |
Authors of publication | Ebner, Fabian; Greb, Lutz |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2018 |
Journal volume | 140 |
Journal issue | 50 |
Pages of publication | 17409 - 17412 |
a | 9.009 ± 0.0018 Å |
b | 13.671 ± 0.003 Å |
c | 11.931 ± 0.002 Å |
α | 90° |
β | 108.59 ± 0.03° |
γ | 90° |
Cell volume | 1392.8 ± 0.5 Å3 |
Cell temperature | 120 K |
Ambient diffraction temperature | 120 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1427 |
Residual factor for significantly intense reflections | 0.065 |
Weighted residual factors for significantly intense reflections | 0.1177 |
Weighted residual factors for all reflections included in the refinement | 0.1454 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.015 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
243314 (current) | 2019-11-26 | cif/ Adding structures of 4133557 via cif-deposit CGI script. |
4133557.cif |
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