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Information card for entry 4134752
Preview
| Coordinates | 4134752.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H59 Cl O3 Si2 |
|---|---|
| Calculated formula | C33 H59 Cl O3 Si2 |
| Title of publication | Asymmetric Total Synthesis of (-)-Spirochensilide A. |
| Authors of publication | Liang, Xin-Ting; Chen, Jia-Hua; Yang, Zhen |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2020 |
| a | 10.9749 ± 0.0003 Å |
| b | 24.6837 ± 0.0008 Å |
| c | 13.5232 ± 0.0004 Å |
| α | 90° |
| β | 95.884 ± 0.003° |
| γ | 90° |
| Cell volume | 3644.15 ± 0.19 Å3 |
| Cell temperature | 104.6 K |
| Ambient diffraction temperature | 104.6 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0782 |
| Residual factor for significantly intense reflections | 0.0526 |
| Weighted residual factors for significantly intense reflections | 0.1033 |
| Weighted residual factors for all reflections included in the refinement | 0.1141 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 250937 (current) | 2020-04-20 | cif/ Adding structures of 4134752 via cif-deposit CGI script. |
4134752.cif |
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