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Information card for entry 4134753
Preview
| Coordinates | 4134753.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H58 O3 Si2 |
|---|---|
| Calculated formula | C33 H58 O3 Si2 |
| Title of publication | Asymmetric Total Synthesis of (-)-Spirochensilide A. |
| Authors of publication | Liang, Xin-Ting; Chen, Jia-Hua; Yang, Zhen |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2020 |
| a | 7.3602 ± 0.0005 Å |
| b | 17.1118 ± 0.0011 Å |
| c | 26.8552 ± 0.0016 Å |
| α | 93.828 ± 0.005° |
| β | 96.178 ± 0.005° |
| γ | 92.265 ± 0.005° |
| Cell volume | 3351.4 ± 0.4 Å3 |
| Cell temperature | 106.4 K |
| Ambient diffraction temperature | 106.4 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1769 |
| Residual factor for significantly intense reflections | 0.0824 |
| Weighted residual factors for significantly intense reflections | 0.114 |
| Weighted residual factors for all reflections included in the refinement | 0.147 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.99 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 250938 (current) | 2020-04-20 | cif/ Adding structures of 4134753 via cif-deposit CGI script. |
4134753.cif |
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