Crystallography Open Database

Information card for entry 4303967

Preview

Coordinates	4303967.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H63 Cl6 Ga3 O3 Si3
Calculated formula	C33 H63 Cl6 Ga3 O3 Si3
Title of publication	Hydrogallation of Alkynes with H-GaCl2: Formation of Organoelement Dichlorogallium Compounds Potentially Applicable as Chelating Lewis Acids
Authors of publication	Werner Uhl; Michael Claesener
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4463 - 4470
a	25.142 ± 0.01 Å
b	13.559 ± 0.005 Å
c	28.259 ± 0.011 Å
α	90°
β	90°
γ	90°
Cell volume	9634 ± 6 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0939
Residual factor for significantly intense reflections	0.051
Weighted residual factors for significantly intense reflections	0.0915
Weighted residual factors for all reflections included in the refinement	0.1026
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179077 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/39.	4303967.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303967.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303967.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4303967.cif