Crystallography Open Database

Information card for entry 4303968

Preview

Coordinates	4303968.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H62 Cl2 Ga2 O2 Si4
Calculated formula	C34 H62 Cl2 Ga2 O2 Si4
Title of publication	Hydrogallation of Alkynes with H-GaCl2: Formation of Organoelement Dichlorogallium Compounds Potentially Applicable as Chelating Lewis Acids
Authors of publication	Werner Uhl; Michael Claesener
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4463 - 4470
a	13.73 ± 0.003 Å
b	10.345 ± 0.002 Å
c	16.897 ± 0.004 Å
α	90°
β	112.335 ± 0.004°
γ	90°
Cell volume	2219.9 ± 0.8 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0588
Residual factor for significantly intense reflections	0.04
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.1017
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179077 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/39.	4303968.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303968.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303968.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4303968.cif