Crystallography Open Database

Information card for entry 4304960

Preview

Coordinates	4304960.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17.2 H33.4 B2 Cl4.4 N7
Calculated formula	C17.2 H33.4 B2 Cl4.4 N7
Title of publication	First Dinuclear B(II) Monocations with Bridging Guanidinate Ligands: Synthesis and Properties
Authors of publication	Oxana Ciobanu; Dimitri Emeljanenko; Elisabeth Kaifer; Jürgen Mautz; Hans-Jörg Himmel
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4774 - 4778
a	10.579 ± 0.002 Å
b	29.517 ± 0.006 Å
c	16.602 ± 0.003 Å
α	90°
β	96.73 ± 0.03°
γ	90°
Cell volume	5148.4 ± 1.7 Å³
Cell temperature	200 K
Ambient diffraction temperature	200 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1451
Residual factor for significantly intense reflections	0.0753
Weighted residual factors for significantly intense reflections	0.2065
Weighted residual factors for all reflections included in the refinement	0.2507
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4304960.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304960.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304960.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304960.cif