Crystallography Open Database

Information card for entry 4304961

Preview

Coordinates	4304961.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H39 B2 Cl3 N8
Calculated formula	C19 H39 B2 Cl3 N8
Title of publication	First Dinuclear B(II) Monocations with Bridging Guanidinate Ligands: Synthesis and Properties
Authors of publication	Oxana Ciobanu; Dimitri Emeljanenko; Elisabeth Kaifer; Jürgen Mautz; Hans-Jörg Himmel
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4774 - 4778
a	9.859 ± 0.002 Å
b	10.313 ± 0.002 Å
c	14.883 ± 0.003 Å
α	74.73 ± 0.03°
β	83.49 ± 0.03°
γ	62.6 ± 0.03°
Cell volume	1296 ± 0.6 Å³
Cell temperature	200 K
Ambient diffraction temperature	200 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0993
Residual factor for significantly intense reflections	0.0635
Weighted residual factors for significantly intense reflections	0.1626
Weighted residual factors for all reflections included in the refinement	0.1965
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179087 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/49.	4304961.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304961.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304961.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304961.cif