Crystallography Open Database

Information card for entry 4308538

Preview

Coordinates	4308538.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C9 H36 N9 S4 Sb Sm
Calculated formula	C9 H34 N9 S4 Sb Sm
Title of publication	The First Example of Solvothermally Synthesized Thioantimonates(V) with Ethylenediamine Coordinated Lanthanide(III): [Sm(en)4]SbS4.0.5en and [Sm(en)3(H2O)(μ-SbS4)]\ιnfty
Authors of publication	Ding-xian Jia; Qin-Yu Zhu; Jie Dai; Wen Lu; Wen-Juan Guo
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	819 - 821
a	11.052 ± 0.0013 Å
b	12.8847 ± 0.0015 Å
c	16.116 ± 0.002 Å
α	90°
β	91.861 ± 0.003°
γ	90°
Cell volume	2293.7 ± 0.5 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0326
Residual factor for significantly intense reflections	0.03
Weighted residual factors for significantly intense reflections	0.0598
Weighted residual factors for all reflections included in the refinement	0.0605
Goodness-of-fit parameter for all reflections included in the refinement	1.255
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4308538.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4308538.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308538.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4308538.cif