Crystallography Open Database

Information card for entry 4308539

Preview

Coordinates	4308539.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 H26 N6 O S4 Sb Sm
Calculated formula	C6 H16 N6 O S4 Sb Sm
Title of publication	The First Example of Solvothermally Synthesized Thioantimonates(V) with Ethylenediamine Coordinated Lanthanide(III): [Sm(en)4]SbS4.0.5en and [Sm(en)3(H2O)(μ-SbS4)]\ιnfty
Authors of publication	Ding-xian Jia; Qin-Yu Zhu; Jie Dai; Wen Lu; Wen-Juan Guo
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	819 - 821
a	9.2725 ± 0.0006 Å
b	13.3851 ± 0.0009 Å
c	14.6863 ± 0.0009 Å
α	90°
β	90°
γ	90°
Cell volume	1822.8 ± 0.2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0221
Residual factor for significantly intense reflections	0.0214
Weighted residual factors for significantly intense reflections	0.0499
Weighted residual factors for all reflections included in the refinement	0.0503
Goodness-of-fit parameter for all reflections included in the refinement	1.149
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4308539.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4308539.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308539.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4308539.cif