Crystallography Open Database

Information card for entry 4309246

Preview

Coordinates	4309246.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C77 H66 Cl2 N12 Rh2
Calculated formula	C77 H66 Cl2 N12 Rh2
Title of publication	Photoinduced One-Electron Reduction of Alkyl Halides by Dirhodium(II,II) Tetraformamidinates and a Related Complex with Visible Light
Authors of publication	Daniel A. Lutterman; Natalya N. Degtyareva; Dean H. Johnston; Judith C. Gallucci; Judith L. Eglin; Claudia Turro
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	5388 - 5396
a	18.5107 ± 0.0003 Å
b	21.7505 ± 0.0004 Å
c	16.6588 ± 0.0003 Å
α	90°
β	96.433 ± 0.001°
γ	90°
Cell volume	6664.9 ± 0.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0597
Residual factor for significantly intense reflections	0.0369
Weighted residual factors for all reflections	0.0935
Weighted residual factors for all reflections included in the refinement	0.0851
Goodness-of-fit parameter for all reflections	1.04
Goodness-of-fit parameter for all reflections included in the refinement	1.096
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179130 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/92.	4309246.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4309246.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4309246.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4309246.cif