Crystallography Open Database

Information card for entry 4309253

Preview

Coordinates	4309253.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H50 N4 Sb2
Calculated formula	C52 H50 N4 Sb2
SMILES	c1(ccccc1)[Sb]1(NCc2ccccc2)(N(Cc2ccccc2)[Sb](c2ccccc2)(c2ccccc2)(NCc2ccccc2)N1Cc1ccccc1)c1ccccc1
Title of publication	Synthetic and Structural Studies of Cyclodistib(V)azanes
Authors of publication	May C. Copsey; Sabrina B. Gallon; Sara K. Grocott; John C. Jeffery; Christopher A. Russell; John M. Slattery
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	5495 - 5500
a	11.9894 ± 0.0015 Å
b	17.422 ± 0.002 Å
c	10.3495 ± 0.0013 Å
α	90°
β	92.874 ± 0.002°
γ	90°
Cell volume	2159.1 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0328
Residual factor for significantly intense reflections	0.0209
Weighted residual factors for significantly intense reflections	0.0475
Weighted residual factors for all reflections included in the refinement	0.0645
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179130 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/92.	4309253.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4309253.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4309253.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4309253.cif