Crystallography Open Database

Information card for entry 4309254

Preview

Coordinates	4309254.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H49 N2 O3 Sb
Calculated formula	C38 H49 N2 O3 Sb
Title of publication	Synthetic and Structural Studies of Cyclodistib(V)azanes
Authors of publication	May C. Copsey; Sabrina B. Gallon; Sara K. Grocott; John C. Jeffery; Christopher A. Russell; John M. Slattery
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	5495 - 5500
a	10.6394 ± 0.0013 Å
b	11.3319 ± 0.0014 Å
c	15.5579 ± 0.0019 Å
α	77.251 ± 0.002°
β	75.6 ± 0.002°
γ	84.373 ± 0.002°
Cell volume	1770.2 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0706
Residual factor for significantly intense reflections	0.0396
Weighted residual factors for significantly intense reflections	0.0805
Weighted residual factors for all reflections included in the refinement	0.0983
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179130 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/92.	4309254.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4309254.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4309254.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4309254.cif