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Information card for entry 4320819
Preview
Coordinates | 4320819.cif |
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Original paper (by DOI) | HTML |
Formula | C19 H24 N6 O3 Si W |
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Calculated formula | C19 H21 N6 O3 Si W |
Title of publication | Syntheses and Structures of Methyltris(pyrazolyl)silane Complexes of the Group 6 Metals |
Authors of publication | Eric E. Pullen; Daniel Rabinovich; Christopher D. Incarvito; Thomas E. Concolino; Arnold L. Rheingold |
Journal of publication | Inorganic Chemistry |
Year of publication | 2000 |
Journal volume | 39 |
Pages of publication | 1561 - 1567 |
a | 18.5761 ± 0.0002 Å |
b | 14.1731 ± 0.0002 Å |
c | 8.4049 ± 0.0002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2212.85 ± 0.07 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P n m a |
Hall space group symbol | -P 2ac 2n |
Residual factor for all reflections | 0.033 |
Residual factor for significantly intense reflections | 0.0289 |
Weighted residual factors for significantly intense reflections | 0.1141 |
Weighted residual factors for all reflections included in the refinement | 0.1221 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
179311 (current) | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/08. |
4320819.cif |
120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4320819.cif |
34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4320819.cif |
18132 | 2011-04-27 | ../uploads/cif-deposit/cod/cif Adding structures of 4320819 via cif-deposit CGI script. |
4320819.cif |
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Users of the data should acknowledge the original authors of the
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