Crystallography Open Database

Information card for entry 4320819

4320818 << 4320819 >> 4320820

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Coordinates	4320819.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H24 N6 O3 Si W
Calculated formula	C19 H21 N6 O3 Si W
Title of publication	Syntheses and Structures of Methyltris(pyrazolyl)silane Complexes of the Group 6 Metals
Authors of publication	Eric E. Pullen; Daniel Rabinovich; Christopher D. Incarvito; Thomas E. Concolino; Arnold L. Rheingold
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	1561 - 1567
a	18.5761 ± 0.0002 Å
b	14.1731 ± 0.0002 Å
c	8.4049 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	2212.85 ± 0.07 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.033
Residual factor for significantly intense reflections	0.0289
Weighted residual factors for significantly intense reflections	0.1141
Weighted residual factors for all reflections included in the refinement	0.1221
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179311 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/08.	4320819.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320819.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320819.cif
18132	2011-04-27	../uploads/cif-deposit/cod/cif Adding structures of 4320819 via cif-deposit CGI script.	4320819.cif