Crystallography Open Database

Information card for entry 4320820

4320819 << 4320820 >> 4320821

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Coordinates	4320820.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H21 Mo N6 O3 Si
Calculated formula	C19 H21 Mo N6 O3 Si
Title of publication	Syntheses and Structures of Methyltris(pyrazolyl)silane Complexes of the Group 6 Metals
Authors of publication	Eric E. Pullen; Daniel Rabinovich; Christopher D. Incarvito; Thomas E. Concolino; Arnold L. Rheingold
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	1561 - 1567
a	18.6624 ± 0.0004 Å
b	14.1761 ± 0.0002 Å
c	8.4402 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	2232.94 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0412
Residual factor for significantly intense reflections	0.0359
Weighted residual factors for significantly intense reflections	0.1269
Weighted residual factors for all reflections included in the refinement	0.1337
Goodness-of-fit parameter for all reflections included in the refinement	1.17
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179311 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/08.	4320820.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320820.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320820.cif
18133	2011-04-27	../uploads/cif-deposit/cod/cif Adding structures of 4320820 via cif-deposit CGI script.	4320820.cif