Crystallography Open Database

Information card for entry 4320821

4320820 << 4320821 >> 4320822

Preview

Coordinates	4320821.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H24 Cr N6 O3 Si
Calculated formula	C19 H21 Cr N6 O3 Si
Title of publication	Syntheses and Structures of Methyltris(pyrazolyl)silane Complexes of the Group 6 Metals
Authors of publication	Eric E. Pullen; Daniel Rabinovich; Christopher D. Incarvito; Thomas E. Concolino; Arnold L. Rheingold
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	1561 - 1567
a	8.0132 ± 0.0006 Å
b	13.7886 ± 0.0009 Å
c	9.6481 ± 0.0007 Å
α	90°
β	97.1566 ± 0.0011°
γ	90°
Cell volume	1057.72 ± 0.13 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0828
Residual factor for significantly intense reflections	0.0638
Weighted residual factors for significantly intense reflections	0.1841
Weighted residual factors for all reflections included in the refinement	0.2041
Goodness-of-fit parameter for all reflections included in the refinement	1.524
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179311 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/08.	4320821.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320821.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320821.cif
18134	2011-04-27	../uploads/cif-deposit/cod/cif Adding structures of 4320821 via cif-deposit CGI script.	4320821.cif