Crystallography Open Database

Information card for entry 4320929

4320928 << 4320929 >> 4320930

Preview

Coordinates	4320929.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H132 Cu3 F7 O9 P6 S2
Calculated formula	C62 H132 Cu3 F7 O9 P6 S2
Title of publication	A Trigonal Planar μ3-Fluorido Coinage Metal Complex from a Dicationic (Diphosphinomethane)copper(I) Dimer: Syntheses, Structures, and Bonding
Authors of publication	Bernd F. Straub; Frank Rominger; Peter Hofmann
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	2113 - 2119
a	21.9548 ± 0.0004 Å
b	16.7994 ± 0.0001 Å
c	23.0086 ± 0.0004 Å
α	90°
β	109.654 ± 0.001°
γ	90°
Cell volume	7991.8 ± 0.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1194
Residual factor for significantly intense reflections	0.0723
Weighted residual factors for significantly intense reflections	0.1673
Weighted residual factors for all reflections included in the refinement	0.1842
Goodness-of-fit parameter for all reflections included in the refinement	1.176
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179312 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/09.	4320929.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320929.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320929.cif
18251	2011-04-28	../uploads/cif-deposit/cod/cif Adding structures of 4320929 via cif-deposit CGI script.	4320929.cif