Crystallography Open Database

Information card for entry 4320930

4320929 << 4320930 >> 4320931

Preview

Coordinates	4320930.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31.5 H66 Cu1.5 F6.5 O1.5 P4
Calculated formula	C31.5 H66 Cu1.5 F6.5 O1.5 P4
Title of publication	A Trigonal Planar μ3-Fluorido Coinage Metal Complex from a Dicationic (Diphosphinomethane)copper(I) Dimer: Syntheses, Structures, and Bonding
Authors of publication	Bernd F. Straub; Frank Rominger; Peter Hofmann
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	2113 - 2119
a	12.2534 ± 0.0001 Å
b	26.2696 ± 0.0002 Å
c	25.2484 ± 0.0002 Å
α	90°
β	90.813 ± 0.001°
γ	90°
Cell volume	8126.44 ± 0.11 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1069
Residual factor for significantly intense reflections	0.0725
Weighted residual factors for significantly intense reflections	0.1863
Weighted residual factors for all reflections included in the refinement	0.2087
Goodness-of-fit parameter for all reflections included in the refinement	1.106
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4320930.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320930.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320930.cif
18252	2011-04-28	../uploads/cif-deposit/cod/cif Adding structures of 4320930 via cif-deposit CGI script.	4320930.cif