Crystallography Open Database

Information card for entry 4321452

Preview

Coordinates	4321452.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H76 O5 P2 Si4 Sm
Calculated formula	C38 H76 O5 P2 Si4 Sm
Title of publication	Synthesis and Structural Characterization of Sm(II) and Yb(II) Complexes Containing Sterically Demanding, Chelating Secondary Phosphide Ligands
Authors of publication	Keith Izod; Paul O'Shaughnessy; Joanne M. Sheffield; William Clegg; Stephen T. Liddle
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	4741 - 4748
a	13.176 ± 0.004 Å
b	13.08 ± 0.004 Å
c	14.546 ± 0.004 Å
α	90°
β	95.363 ± 0.006°
γ	90°
Cell volume	2495.9 ± 1.3 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1251
Residual factor for significantly intense reflections	0.1015
Weighted residual factors for significantly intense reflections	0.2418
Weighted residual factors for all reflections included in the refinement	0.2533
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179317 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/14.	4321452.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321452.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321452.cif
18823	2011-05-04	../uploads/cif-deposit/cod/cif Adding structures of 4321452 via cif-deposit CGI script.	4321452.cif