Crystallography Open Database

Information card for entry 4321453

Preview

Coordinates	4321453.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H70 N2 O P2 Si4 Sm
Calculated formula	C36 H70 N2 O P2 Si4 Sm
Title of publication	Synthesis and Structural Characterization of Sm(II) and Yb(II) Complexes Containing Sterically Demanding, Chelating Secondary Phosphide Ligands
Authors of publication	Keith Izod; Paul O'Shaughnessy; Joanne M. Sheffield; William Clegg; Stephen T. Liddle
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	4741 - 4748
a	14.988 ± 0.0017 Å
b	13.0528 ± 0.0015 Å
c	24.33 ± 0.003 Å
α	90°
β	104.507 ± 0.002°
γ	90°
Cell volume	4608.1 ± 0.9 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0426
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.0854
Weighted residual factors for all reflections included in the refinement	0.0868
Goodness-of-fit parameter for all reflections included in the refinement	1.239
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179317 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/14.	4321453.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321453.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321453.cif
18824	2011-05-04	../uploads/cif-deposit/cod/cif Adding structures of 4321453 via cif-deposit CGI script.	4321453.cif