Crystallography Open Database

Information card for entry 4322021

4322020 << 4322021 >> 4322022

Preview

Coordinates	4322021.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H45 Al Cl2 N4 P2 Si5
Calculated formula	C15 H45 Al Cl2 N4 P2 Si5
SMILES	[Al]1(Cl)(Cl)N(P2P(=[N]1[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)N2[Si](C)(C)C)[Si](C)(C)C
Title of publication	Iminophosphine Cycloaddition Reactions of a Diazaphosphoniaaluminatacyclobutane and a Novel Intramolecular Phosphiridine P\ρightarrowP Coordination
Authors of publication	Neil Burford; Daren J. LeBlanc
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	2248 - 2249
a	22.2416 ± 0.0014 Å
b	8.907 ± 0.0007 Å
c	18.5029 ± 0.0013 Å
α	90°
β	119.528 ± 0.001°
γ	90°
Cell volume	3189.4 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0656
Residual factor for significantly intense reflections	0.0414
Weighted residual factors for significantly intense reflections	0.0836
Weighted residual factors for all reflections included in the refinement	0.091
Goodness-of-fit parameter for all reflections included in the refinement	0.979
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179323 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/20.	4322021.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322021.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322021.cif
19910	2011-05-30	../uploads/cif-deposit/cod/cif Adding structures of 4322021 via cif-deposit CGI script.	4322021.cif