Crystallography Open Database

Information card for entry 4322022

4322021 << 4322022 >> 4322023

Preview

Coordinates	4322022.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H56 Al Cl2 N4 P3 Si4
Calculated formula	C36 H56 Al Cl2 N4 P3 Si4
Title of publication	Iminophosphine Cycloaddition Reactions of a Diazaphosphoniaaluminatacyclobutane and a Novel Intramolecular Phosphiridine P\ρightarrowP Coordination
Authors of publication	Neil Burford; Daren J. LeBlanc
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	2248 - 2249
a	14.6485 ± 0.0003 Å
b	18.6224 ± 0.0004 Å
c	17.3207 ± 0.0004 Å
α	90°
β	98.626 ± 0.001°
γ	90°
Cell volume	4671.47 ± 0.18 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0798
Residual factor for significantly intense reflections	0.0457
Weighted residual factors for significantly intense reflections	0.1212
Weighted residual factors for all reflections included in the refinement	0.1361
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179323 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/20.	4322022.cif
131580	2015-02-08	cif/ (antanas@koala.ibt.lt) Replacing typo ".." values with ".".	4322022.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322022.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322022.cif
19911	2011-05-30	../uploads/cif-deposit/cod/cif Adding structures of 4322022 via cif-deposit CGI script.	4322022.cif