Crystallography Open Database

Information card for entry 4323581

Preview

Coordinates	4323581.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H5 N O9 Os3 S
Calculated formula	C15 H5 N O9 Os3 S
Title of publication	Reactions of Triosmium Carbonyl Clusters with Thionylaniline. Crystal Structures of Os~3~(CO)~9~(μ~3~-NPh)(μ~3~-S), Os~3~(CO)~9~(μ~3~,η^2^-(PhN)~2~SO)(μ~3~-S), and Os~3~(CO)~8~(NCMe)(μ~3~-NPh)(μ~3~-S).
Authors of publication	Wen-Yann Yeh; Charlotte L. Stern; Duward F. Shriver
Journal of publication	Inorganic Chemistry
Year of publication	1997
Journal volume	36
Pages of publication	4408 - 4414
a	16.603 ± 0.007 Å
b	8.679 ± 0.004 Å
c	29.009 ± 0.006 Å
α	90°
β	102.08 ± 0.02°
γ	90°
Cell volume	4088 ± 3 Å³
Cell temperature	153.2 K
Ambient diffraction temperature	153.2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0356
Weighted residual factors for significantly intense reflections	0.039
Goodness-of-fit parameter for significantly intense reflections	2.047
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4323581.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4323581.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4323581.cif
23829	2011-08-11	../uploads/cif-deposit/cod/cif Adding structures of 4323581 via cif-deposit CGI script.	4323581.cif