Crystallography Open Database

Information card for entry 4323582

Preview

Coordinates	4323582.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H10 N2 O10 Os3 S2
Calculated formula	C21 H10 N2 O10 Os3 S2
Title of publication	Reactions of Triosmium Carbonyl Clusters with Thionylaniline. Crystal Structures of Os~3~(CO)~9~(μ~3~-NPh)(μ~3~-S), Os~3~(CO)~9~(μ~3~,η^2^-(PhN)~2~SO)(μ~3~-S), and Os~3~(CO)~8~(NCMe)(μ~3~-NPh)(μ~3~-S).
Authors of publication	Wen-Yann Yeh; Charlotte L. Stern; Duward F. Shriver
Journal of publication	Inorganic Chemistry
Year of publication	1997
Journal volume	36
Pages of publication	4408 - 4414
a	9.723 ± 0.004 Å
b	15.704 ± 0.004 Å
c	18.455 ± 0.007 Å
α	113.17 ± 0.03°
β	102.48 ± 0.03°
γ	89.97 ± 0.03°
Cell volume	2518.2 ± 1.7 Å³
Cell temperature	153.2 K
Ambient diffraction temperature	153.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0298
Weighted residual factors for significantly intense reflections	0.0255
Goodness-of-fit parameter for significantly intense reflections	1.312
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4323582.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4323582.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4323582.cif
23830	2011-08-11	../uploads/cif-deposit/cod/cif Adding structures of 4323582 via cif-deposit CGI script.	4323582.cif