Crystallography Open Database

Information card for entry 4324239

Preview

Coordinates	4324239.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H90 Li N6 O6 U
Calculated formula	C42 H60 Li N6 O6 U
Title of publication	Comparison of the Redox Chemistry of Primary and Secondary Amides of U(IV): Isolation of a U(VI) Bis(imido) Complex or a Homoleptic U(VI) Amido Complex
Authors of publication	Lani A. Seaman; Skye Fortier; Guang Wu; Trevor W. Hayton
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	636 - 646
a	15.1725 ± 0.0014 Å
b	18.7754 ± 0.0017 Å
c	17.1225 ± 0.0015 Å
α	90°
β	92.492 ± 0.001°
γ	90°
Cell volume	4873.1 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0678
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.1254
Weighted residual factors for all reflections included in the refinement	0.1358
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179345 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/42.	4324239.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324239.cif
40944	2012-03-09	../uploads/cif-deposit/cod/cif Adding structures of 4324239 via cif-deposit CGI script.	4324239.cif