Crystallography Open Database

Information card for entry 4324240

Preview

Coordinates	4324240.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Uranium(VI) Piperidide
Formula	C30 H60 N6 U
Calculated formula	C30 H60 N6 U
SMILES	C1CCCN([U](N2CCCCC2)(N2CCCCC2)(N2CCCCC2)(N2CCCCC2)N2CCCCC2)C1
Title of publication	Comparison of the Redox Chemistry of Primary and Secondary Amides of U(IV): Isolation of a U(VI) Bis(imido) Complex or a Homoleptic U(VI) Amido Complex
Authors of publication	Lani A. Seaman; Skye Fortier; Guang Wu; Trevor W. Hayton
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	636 - 646
a	10.386 ± 0.0013 Å
b	17.154 ± 0.002 Å
c	17.858 ± 0.002 Å
α	90°
β	100.896 ± 0.002°
γ	90°
Cell volume	3124.2 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0628
Residual factor for significantly intense reflections	0.0364
Weighted residual factors for significantly intense reflections	0.0778
Weighted residual factors for all reflections included in the refinement	0.0865
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179345 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/42.	4324240.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324240.cif
40945	2012-03-09	../uploads/cif-deposit/cod/cif Adding structures of 4324240 via cif-deposit CGI script.	4324240.cif