Crystallography Open Database

Information card for entry 4325106

Preview

Coordinates	4325106.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	apx979
Formula	C34 H57 I2 N3 O3 U
Calculated formula	C34 H57 I2 N3 O3 U
Title of publication	A General and Modular Synthesis of Monoimidouranium(IV) Dihalides
Authors of publication	Robert E. Jilek; Liam P. Spencer; David L. Kuiper; Brian L. Scott; Ursula J. Williams; James M. Kikkawa; Eric J. Schelter; James M. Boncella
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	4235 - 4237
a	11.253 ± 0.002 Å
b	12.979 ± 0.003 Å
c	14.875 ± 0.003 Å
α	114.51 ± 0.03°
β	93.85 ± 0.03°
γ	90.03 ± 0.03°
Cell volume	1971.3 ± 0.8 Å³
Cell temperature	140 ± 1 K
Ambient diffraction temperature	140 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0679
Residual factor for significantly intense reflections	0.0389
Weighted residual factors for significantly intense reflections	0.0738
Weighted residual factors for all reflections included in the refinement	0.0803
Goodness-of-fit parameter for all reflections included in the refinement	0.884
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179354 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/51.	4325106.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325106.cif
43558	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4325106 via cif-deposit CGI script.	4325106.cif