Crystallography Open Database

Information card for entry 4325107

Preview

Coordinates	4325107.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H66 Cl4 N2 O4 U2
Calculated formula	C40 H66 Cl4 N2 O4 U2
Title of publication	A General and Modular Synthesis of Monoimidouranium(IV) Dihalides
Authors of publication	Robert E. Jilek; Liam P. Spencer; David L. Kuiper; Brian L. Scott; Ursula J. Williams; James M. Kikkawa; Eric J. Schelter; James M. Boncella
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	4235 - 4237
a	16.386 ± 0.004 Å
b	15.896 ± 0.004 Å
c	17.234 ± 0.004 Å
α	90°
β	96.288 ± 0.003°
γ	90°
Cell volume	4462 ± 1.9 Å³
Cell temperature	140 ± 1 K
Ambient diffraction temperature	140 ± 1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1033
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.1143
Weighted residual factors for all reflections included in the refinement	0.1423
Goodness-of-fit parameter for all reflections included in the refinement	0.955
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179354 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/51.	4325107.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325107.cif
43559	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4325107 via cif-deposit CGI script.	4325107.cif