Crystallography Open Database

Information card for entry 4327478

Preview

Coordinates	4327478.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C145.2 H151.2 Ag5 I5 O14.3 P4
Calculated formula	C145.2 H151.2 Ag5 I5 O14.3 P4
Title of publication	Tetraphosphinitoresorcinarene Complexes: Dynamic Clusters with Silver(I) and Copper(I) Halides
Authors of publication	Dana J. Eisler; Christopher W. Kirby; Richard J. Puddephatt
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	7626 - 7634
a	15.9824 ± 0.0001 Å
b	25.2649 ± 0.0001 Å
c	35.4313 ± 0.0001 Å
α	90°
β	101.705 ± 0.001°
γ	90°
Cell volume	14009.4 ± 0.12 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0808
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for significantly intense reflections	0.1112
Weighted residual factors for all reflections included in the refinement	0.1248
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4327478.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327478.cif
61279	2012-06-26	cif/4 Fixing wrong year of publication of several entries (there was a mistake when these files were deposited)	4327478.cif
61249	2012-06-25	cif/ Adding structures of 4327478 via cif-deposit CGI script.	4327478.cif