Crystallography Open Database

Information card for entry 4327479

Preview

Coordinates	4327479.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C143 H118 Ag5 Cl9 I5 O13.5 P4
Calculated formula	C143 H118 Ag5 Cl9 I5 O13.5 P4
Title of publication	Tetraphosphinitoresorcinarene Complexes: Dynamic Clusters with Silver(I) and Copper(I) Halides
Authors of publication	Dana J. Eisler; Christopher W. Kirby; Richard J. Puddephatt
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	7626 - 7634
a	19.3247 ± 0.0002 Å
b	22.8616 ± 0.0004 Å
c	19.7339 ± 0.0003 Å
α	90°
β	117.315 ± 0.001°
γ	90°
Cell volume	7746.2 ± 0.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.1312
Residual factor for significantly intense reflections	0.088
Weighted residual factors for significantly intense reflections	0.272
Weighted residual factors for all reflections included in the refinement	0.3103
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4327479.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327479.cif
61279	2012-06-26	cif/4 Fixing wrong year of publication of several entries (there was a mistake when these files were deposited)	4327479.cif
61250	2012-06-25	cif/ Adding structures of 4327479 via cif-deposit CGI script.	4327479.cif